2-Propenoic acid, 3-[3-(chlorosulfonyl)phenyl]-, Methyl ester, (2E)- synthesis
- Product Name:2-Propenoic acid, 3-[3-(chlorosulfonyl)phenyl]-, Methyl ester, (2E)-
- CAS Number:610801-83-7
- Molecular formula:C10H9ClO4S
- Molecular Weight:260.69
58186-45-1
18 suppliers
$243.00/1g
610801-83-7
22 suppliers
$348.48/1g
Yield:-
Reaction Conditions:
Stage #1: 3-(3-amino-phenyl)-acrylic acid methyl esterwith hydrogenchloride;glacial acetic acid in lithium hydroxide monohydrate;
Stage #2: with NaNO2 in lithium hydroxide monohydrate at -13 - -5;
Stage #3: with sulfur(IV) oxide;glacial acetic acid;copper chloride (I) in lithium hydroxide monohydrate at 0;
References:
Yang, Lei;Xue, Xiaowen;Zhang, Yihua [Synthetic Communications,2010,vol. 40,# 17,p. 2520 - 2524] Location in patent:experimental part
100-52-7
953 suppliers
$21.30/2g
610801-83-7
22 suppliers
$348.48/1g
99-61-6
651 suppliers
$5.00/10g
610801-83-7
22 suppliers
$348.48/1g
659-04-1
34 suppliers
inquiry
610801-83-7
22 suppliers
$348.48/1g
555-68-0
170 suppliers
$10.00/1g
610801-83-7
22 suppliers
$348.48/1g