6-CHLOROINDOLE-3-ACETONITRILE synthesis
- Product Name:6-CHLOROINDOLE-3-ACETONITRILE
- CAS Number:61220-58-4
- Molecular formula:C10H7ClN2
- Molecular Weight:190.63
773837-37-9
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17422-33-2
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74-88-4
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Yield:-
Reaction Conditions:
Stage #1: 6-chloroindolewith eschenmoser's salt;acetic acid in acetonitrile at 20; for 4 h;
Stage #2: methyl iodide in ethanol at 20; for 18 h;
Stage #3: sodium cyanide in water;N,N-dimethyl-formamide at 70; for 4 h;
References:
Egami, Hiromichi;Hotta, Ryo;Otsubo, Minami;Rouno, Taiki;Niwa, Tomoki;Yamashita, Kenji;Hamashima, Yoshitaka [Organic Letters,2020,vol. 22,# 14,p. 5656 - 5660] Location in patent:supporting information
17422-33-2
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$10.00/1g
61220-58-4
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