6,2'-DIBROMO-[3,4']-BIPYRIDINE synthesis
- Product Name:6,2'-DIBROMO-[3,4']-BIPYRIDINE
- CAS Number:942206-16-8
- Molecular formula:C10H6Br2N2
- Molecular Weight:313.98
100523-96-4
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$8.00/1g
223463-14-7
246 suppliers
$6.00/250mg
942206-16-8
9 suppliers
$105.00/100mg
Yield:942206-16-8 41%
Reaction Conditions:
Stage #1: 2-bromo-4-iodopyridine;6-bromopyridin-3-ylboronic acidwith tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran at 50; for 1 h;Inert atmosphere;Suzuki-Miyaura Coupling;
Stage #2: with sodium carbonate in tetrahydrofuran;water at 50; for 12 h;Inert atmosphere;Suzuki-Miyaura Coupling;
References:
Okazawa, Atsushi;Terakado, Yutaro;Ishida, Takayuki;Kojima, Norimichi [New Journal of Chemistry,2018,vol. 42,# 22,p. 17874 - 17878] Location in patent:supporting information
58530-53-3
303 suppliers
$4.00/1g
223463-14-7
246 suppliers
$6.00/250mg
![4,6'-DIBROMO-[2,3']-BIPYRIDINE](/CAS/GIF/942206-14-6.gif)
942206-14-6
5 suppliers
$105.00/100mg
942206-16-8
9 suppliers
$105.00/100mg