3-METHYL-1,3,4,5-TETRAHYDRO-BENZO[B][1,4]DIAZEPIN-2-ONE synthesis
- Product Name:3-METHYL-1,3,4,5-TETRAHYDRO-BENZO[B][1,4]DIAZEPIN-2-ONE
- CAS Number:54028-76-1
- Molecular formula:C10H12N2O
- Molecular Weight:176.22
88-74-4
10 suppliers
$10.00/1g
54028-76-1
25 suppliers
$45.00/25mg
Yield:-
Steps:
Multi-step reaction with 2 steps
1: sulfuric acid / 80 °C
2: zinc; phosphoric acid / 1,4-dioxane / 110 °C
References:
Tabata, Hidetsugu;Tsuji, Yuka;Yoneda, Tetsuya;Tasaka, Tomohiko;Oshitari, Tetsuta;Takahashi, Hideyo;Natsugari, Hideaki [Synlett,2018,vol. 29,# 16,p. 2141 - 2146]
