5'-noraristeromycin synthesis

4synthesis methods

Product Name:5'-noraristeromycin
CAS Number:142635-42-5
Molecular formula:C10H13N5O3
Molecular Weight:251.2419

88756-83-6 Synthesis

88756-83-6
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142635-42-5
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 85 percent / Et₃N / butan-1-ol / 40 h / 120 °C
2: 2.) HCl / 1.) a) RT, 1 h, b) 80 to 90 deg C, 40 h, 2.) MeOH, RT, 30 min
3: 65 percent / NH₃ / methanol / 48 h / 140 °C

References:

Patil, Sharadbala D.;Schneller, Stewart W.;Hosoya, Mitsuaki;Snoeck, Robert;Andrei, Graciela;et al. [Journal of Medicinal Chemistry,1992,vol. 35,# 18,p. 3372 - 3377]

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4H-Cyclopenta-1,3-dioxol-4-ol, 6-[(5-amino-6-chloro-4-pyrimidinyl)amino]tetrahydro-2,2-dimethyl-, (3aR,4S,6R,6aS)-rel-

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142635-42-5
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2-Cyclopenten-1-ol, 4-(6-amino-9H-purin-9-yl)-, (1R,4S)-rel-

111189-91-4
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142635-42-5
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References