5-METHYL-[1'-13C]URIDINE synthesis
- Product Name:5-METHYL-[1'-13C]URIDINE
- CAS Number:201996-60-3
- Molecular formula:C10H14N2O6
- Molecular Weight:259.24
380611-22-3
1 suppliers
inquiry
201996-60-3
17 suppliers
$165.00/5mg
Yield:-
Steps:
Multi-step reaction with 4 steps
1: 95 percent / BF3*Et2O / CH2Cl2 / 1 h / 0 °C
2: 95 percent / m-CPBA, NaHCO3 / CH2Cl2 / 1 h / 0 °C
3: 1) hexamethyldisilazane, 2) TMSOTf / 1) 2 h, reflux, 2) 1,2-dichloroethane, 5 min, r.t.
4: 2M NaOH, pyridine / methanol / 0.08 h / 0 °C
References:
Chanteloup, Luc;Beau, Jean-Marie [Tetrahedron Letters,1992,vol. 33,# 37,p. 5347 - 5350]