ChemicalBook CAS DataBase List (2R,3S,4S,5R)-2,5-Bis(hydroxymethyl)-oxolane-2,3,4-triol

(2R,3S,4S,5R)-2,5-Bis(hydroxymethyl)-oxolane-2,3,4-triol synthesis

7synthesis methods

Product Name:(2R,3S,4S,5R)-2,5-Bis(hydroxymethyl)-oxolane-2,3,4-triol
CAS Number:470-23-5
Molecular formula:C6H12O6
Molecular Weight:180.16

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(2R,3S,4S,5R)-2,5-Bis(hydroxymethyl)-oxolane-2,3,4-triol

470-23-5
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Yield:-

Reaction Conditions:

with sodium aluminate in water monomer;dimethyl sulfoxide at 55; for 3 h;Solvent;Concentration;

Steps:

2.2.2 General procedure for the isomerization of D-glucose syrup into D-fructose

A round bottom glass flask equipped with a magnetic bar was charged with a syrup of D-glucose (10g, 70% dry matter) and solvents. After stirring at 55°C till dissolution of D-glucose, the catalyst was added and resulting mixture was stirred at 55°C for 3h.

References:

Despax, Solenne;Estrine, Boris;Hoffmann, Norbert;Le Bras, Jean;Marinkovic, Sinisa;Muzart, Jacques [Catalysis Communications,2013,vol. 39,p. 35 - 38]