8-methoxy-2-methyl-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole synthesis
- Product Name:8-methoxy-2-methyl-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole
- CAS Number:41505-84-4
- Molecular formula:C13H16N2O
- Molecular Weight:216.28
923293-14-5
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Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: acetic acid; sodium nitrite / water / 1.5 h / 0 °C / Inert atmosphere
1.2: 0 - 20 °C / Inert atmosphere
2.1: dichloromethane / 20 °C / Inert atmosphere
3.1: ruthenium trichloride hydrate / Isopropyl acetate / 15 h / 80 °C / Inert atmosphere
4.1: sodium tetrahydroborate / methanol; water / 20 - 100 °C / Inert atmosphere
References:
Dong, Huijun;Latka, Regina T.;Driver, Tom G. [Organic Letters,2011,vol. 13,# 10,p. 2726 - 2729]
1346446-48-7
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![1H-Pyrido[4,3-b]indol-1-one, 2,3,4,5-tetrahydro-8-methoxy-2-methyl-](/CAS/20210305/GIF/1426943-74-9.gif)
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41505-84-4
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1445-73-4
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3471-32-7
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19501-58-7
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41505-84-4
10 suppliers
$45.00/50mg