4-TERT-BUTYL-2,6-DIFORMYLPHENOL synthesis
- Product Name:4-TERT-BUTYL-2,6-DIFORMYLPHENOL
- CAS Number:84501-28-0
- Molecular formula:C12H14O3
- Molecular Weight:206.24
2203-14-7
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84501-28-0
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$75.00/50mg
Yield:84501-28-0 77%
Reaction Conditions:
with manganese(IV) oxide in chloroform for 8 h;Reflux;
Steps:
Compound 2:
Activated MnO2 (40 g) was added to CHCl3 (200 mL) in a 500 mL round bottom flask. The mixture was heated to reflux with stirring about 15 min, then the powder of compound 3 (5.0 g) was added. After being kept refluxing for 8 h, the reaction mixture was cooled to room temperature and filtered. The solid was washed by CHCl3 (40 mL x 5) thoroughly until the filtrate was colorless. Then the filtrate was concentrated on a rotary evaporator yielding a yellow solid (3.8 g, 77% yield),
References:
Zhu, Chengjian;Fu, Yong;Xing, Zhitao;Zhu, Chengcheng;Yang, Hongwei;He, Weijiang;Cheng, Yixiang [Tetrahedron Letters,2012,vol. 53,# 7,p. 804 - 807] Location in patent:supporting information; experimental part
98-54-4
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100-97-0
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$14.00/250G
84501-28-0
78 suppliers
$75.00/50mg
98-54-4
424 suppliers
$15.00/25g
84501-28-0
78 suppliers
$75.00/50mg
50-00-0
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$10.00/25g
98-54-4
424 suppliers
$15.00/25g
84501-28-0
78 suppliers
$75.00/50mg