4-Methoxycyclohexanol synthesis
- Product Name:4-Methoxycyclohexanol
- CAS Number:18068-06-9
- Molecular formula:C7H14O2
- Molecular Weight:130.18
![1,4-Dioxaspiro[4.5]decan-8-one](/CAS/GIF/4746-97-8.gif)
4746-97-8
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18068-06-9
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$22.00/250mg
Yield:-
Steps:
Multi-step reaction with 4 steps
1: 98 percent / NaBH4 / methanol / 1.) 0 deg C, 0.5 h, 2.) room temperature, 1 h
2: 81 percent / KOH / dimethylsulfoxide / Ambient temperature
3: 85 percent / oxalic acid / CH2Cl2; H2O / Ambient temperature
4: NaBH4 / methanol / 0 - 20 °C
References:
Shvily, Ronit;Mueller, Thomas;Apeloig, Yitzhak;Mandelbaum, Asher [Journal of the Chemical Society. Perkin Transactions 2 (2001),1997,# 6,p. 1221 - 1234]
150-76-5
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18068-06-9
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$22.00/250mg
556-48-9
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74-88-4
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18068-06-9
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150-76-5
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18068-06-9
95 suppliers
$22.00/250mg
108-93-0
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150-76-5
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18068-06-9
95 suppliers
$22.00/250mg
69125-55-9
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