4-Cyanobenzoyl chloride synthesis
- Product Name:4-Cyanobenzoyl chloride
- CAS Number:6068-72-0
- Molecular formula:C8H4ClNO
- Molecular Weight:165.58
619-65-8
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6068-72-0
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Yield:6068-72-0 98%
Steps:
62 Example 62
After dry nitrogen gas was introduced to the reaction mixture for one hour, acetonitrile was removed under ambient pressure, and was further removed under reduced pressure through distillation, to thereby obtain 16.2 g of p-cyanobenzoyl chloride (yield 98%, based on p-cyanobenzoic acid). The p-cyanobenzoyl chloride obtained had a purity of 99%.
References:
Showa Denko Kabushiki Kaisha US6433211, 2002, B1
1877-72-1
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6068-72-0
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1711-11-1
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3058-39-7
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122-04-3
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636-98-6
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6068-72-0
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6068-72-0
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