4-CHLORO-2-ANISIDINE HYDROCHLORIDE synthesis
- Product Name:4-CHLORO-2-ANISIDINE HYDROCHLORIDE
- CAS Number:93-50-5
- Molecular formula:C7H8ClNO
- Molecular Weight:157.6
67-56-1
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93-50-5
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Yield: 28%
Reaction Conditions:
with fac-tris(2-phenylpyridinato-N,C2')iridium(III);methanesulfonic acid;triphenylphosphine in acetonitrile at 55; for 24 h;Irradiation;Inert atmosphere;
Steps:
8 Examples 1-16
General procedure: Step 1: Add the nitro compound (see Table 1 for specific substances) and methanol into the reaction vessel, and add the reducing agent (with(See Table 1 for specific substances), photocatalyst (see Table 1 for specific substances), water (see Table 1 for specific materials), organic acids (see Table 1 for specific substances)1) Add the organic solvent (see Table 1 for specific substances) into the reaction vessel.
References:
CN112812027, 2021, A Location in patent:Paragraph 0027; 0030-0032; 0041-0042
6627-53-8
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93-50-5
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90-04-0
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![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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93-50-5
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1092349-89-7
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93-50-5
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