4-CHLORO-2,6-DIPHENYLPYRIMIDINE synthesis
- Product Name:4-CHLORO-2,6-DIPHENYLPYRIMIDINE
- CAS Number:29509-91-9
- Molecular formula:C16H11ClN2
- Molecular Weight:266.72
Yield: 75%
Reaction Conditions:
with tetrakis(triphenylphosphine) palladium(0);tetrabutylammomium bromide;sodium hydroxide in water;toluene at 80; for 12 h;Inert atmosphere;
Steps:
8.1 1) Synthesis of Intermediate 1-38-2:
According to the synthesis method of compound 1-3-3, (12.2g, 100mmol) of compound 1-23-3 and (22.5g, 100mmol) of compound 1-38-1 were substituted for compound 1-3-1 and compound 1- 3-2, the yield is 75%.
References:
Guangzhou Huarui Optoelectric Materials Co., Ltd.;He Ruifeng;Huang Hong;Wu Canjie;Song Jingyao CN111848590, 2020, A Location in patent:Paragraph 0251-0256
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