N1-tert-Butoxycarbonyl 1-(3-Methoxyphenyl)hydrazine synthesis
2synthesis methods
- Product Name:N1-tert-Butoxycarbonyl 1-(3-Methoxyphenyl)hydrazine
- CAS Number:380383-81-3
- Molecular formula:C12H18N2O3
- Molecular Weight:238.28
Yield:380383-81-3 92%
Reaction Conditions:
with copper(l) iodide;caesium carbonate in dimethyl sulfoxide at 50; for 3 h;regioselective reaction;
References:
Jiang, Liqin;Lu, Xu;Zhang, Hui;Jiang, Yongwen;Ma, Dawei [Journal of Organic Chemistry,2009,vol. 74,# 12,p. 4542 - 4546] Location in patent:experimental part