(3-PHENYL-5-ISOXAZOLYL)METHANAMINE synthesis
- Product Name:(3-PHENYL-5-ISOXAZOLYL)METHANAMINE
- CAS Number:54408-35-4
- Molecular formula:C10H10N2O
- Molecular Weight:174.2
90924-12-2
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54408-35-4
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Yield:54408-35-4 78%
Reaction Conditions:
Stage #1: 3-phenyl-5-hydroxymethylisoxazolewith methanesulfonyl chloride;triethylamine in dichloromethane at 20; for 6 h;Cooling;
Stage #2: with sodium azide in N,N-dimethyl-formamide at 55; for 8 h;
Stage #3: with ammonium chloride;zinc in ethanol;water; for 0.5 h;Reflux;
References:
Yin;Jia;Zhao;Xu;Tang;Wang [Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry,2011,vol. 50,# 5,p. 695 - 703] Location in patent:experimental part
942935-99-1
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54408-35-4
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932-90-1
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54408-35-4
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![3,5,7-Triaza-1-azoniatricyclo[3.3.1.13,7]decane, 1-[(3-phenyl-5-isoxazolyl)methyl]-, bromide (1:1)](/CAS/20211123/GIF/66046-44-4.gif)
66046-44-4
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54408-35-4
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$90.00/100mg
100-52-7
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54408-35-4
65 suppliers
$90.00/100mg