3-HYDROXY-2'-METHOXYFLAVONE synthesis
- Product Name:3-HYDROXY-2'-METHOXYFLAVONE
- CAS Number:29219-03-2
- Molecular formula:C16H12O4
- Molecular Weight:268.26
42220-77-9
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29219-03-2
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Yield:29219-03-2 32%
Reaction Conditions:
with dihydrogen peroxide;sodium hydroxide in methanol at 20; for 15 h;
Steps:
2.2.2 Synthesis of the flavanols (step 2)
General procedure: The chalcone was dissolved in 100ml of methanol and 5ml of 30% hydrogen peroxide and sodium hydroxide (1.2g, 30mmol) were added and the mixture was stirred at room temperature for 15h. HCl(c) was added until pH 1 and precipitate formed was filtered under vacuum to obtain the title compound as a solid.
References:
Ravichandran;Singh;Donnelly;Migliore;Johnson;Fishwick;Luke;Martin;Maudsley;Fugmann;Moaddel [Journal of Molecular Graphics and Modelling,2014,vol. 49,p. 38 - 46]
118-93-4
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29219-03-2
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135-02-4
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