3-DEOXY-3-FLUORO-D-GLUCOSE synthesis

3synthesis methods

Product Name:3-DEOXY-3-FLUORO-D-GLUCOSE
CAS Number:14049-03-7
Molecular formula:C6H11FO5
Molecular Weight:182.15

2595-05-3 Synthesis

1,2:5,6-Di-O-isopropylidene-alpha-D-allofuranose

2595-05-3
259 suppliers
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14049-03-7
66 suppliers
$45.00/10 mg

Yield:-

Steps:

Multi-step reaction with 3 steps
1: pyridine / dichloromethane / 1.5 h / -20 °C
2: cesium fluoride / tert-butyl alcohol / 26 h / 80 °C
3: Dowex 50W X₈, H+ / water; 1,4-dioxane / 18 h / 65 °C

References:

Liu, Zilei;Jenkinson, Sarah F.;Vermaas, Tom;Adachi, Isao;Wormald, Mark R.;Hata, Yukako;Kurashima, Yukiko;Kaji, Akira;Yu, Chu-Yi;Kato, Atsushi;Fleet, George W. J. [Journal of Organic Chemistry,2015,vol. 80,# 9,p. 4244 - 4258]

14049-05-9 Synthesis

(3aR,6S,6aS)-5-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)-6-fluoro-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxole

14049-05-9
14 suppliers
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14049-03-7
66 suppliers
$45.00/10 mg

References

α-D-Allofuranose, 1,2:5,6-bis-O-(1-methylethylidene)-, 3-(1,1,1-trifluoromethanesulfonate)

55951-90-1
0 suppliers
inquiry

14049-03-7
66 suppliers
$45.00/10 mg

References

3-DEOXY-3-FLUORO-D-GLUCOSE Related Search:

6-FLUORO-6-DEOXY-D-GLUCOPYRANOSE