3-CHLORO-1-(3,4-DIMETHOXYPHENYL)PROPAN-1-ONE synthesis
- Product Name:3-CHLORO-1-(3,4-DIMETHOXYPHENYL)PROPAN-1-ONE
- CAS Number:4693-38-3
- Molecular formula:C11H13ClO3
- Molecular Weight:228.67
91-16-7
569 suppliers
$13.00/25g
625-36-5
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$45.00/5g
4693-38-3
38 suppliers
$155.00/100mg
Yield:4693-38-3 65.5%
Reaction Conditions:
Stage #1: 2-chloropropionyl chloridewith aluminum (III) chloride in dichloromethane at 20; for 0.5 h;
Stage #2: 1,2-dimethoxybenzene in dichloromethane at 20; for 24 h;
References:
Maqbool, Mudasir;Gadhavi, Joshna;Singh, Anju;Hivare, Pravin;Gupta, Sharad;Hoda, Nasimul [Organic and Biomolecular Chemistry,2021,vol. 19,# 7,p. 1589 - 1603] Location in patent:supporting information