Azetidin-3-ol synthesis
- Product Name:Azetidin-3-ol
- CAS Number:45347-82-8
- Molecular formula:C3H7NO
- Molecular Weight:73.09
141699-55-0
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45347-82-8
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Yield:-
Reaction Conditions:
with trifluoroacetic acid in dichloromethane at 20; for 1 h;
Steps:
U
To a stirred mixture of Λ/-boc-3-hydroxyazetidine (500 mg, 2.89 mmol) in DCM (14 mL) was added trifluoroacetic acid (2.9 mL). The mixture was stirred at room temperature for 1h and concentrated in vacuo to give crude product. This material was mixed with DMF to make a 1 M stock solution and used as is.
References:
BAYER PHARMACEUTICALS CORPORATION WO2007/56170, 2007, A2 Location in patent:Page/Page column 99
18621-17-5
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45347-82-8
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45347-82-8
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45347-82-8
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