3,7-DI(TERT-BUTYL)-1,5-DINITRONAPHTHALENE synthesis
- Product Name:3,7-DI(TERT-BUTYL)-1,5-DINITRONAPHTHALENE
- CAS Number:20870-37-5
- Molecular formula:C18H22N2O4
- Molecular Weight:330.38
91-20-3
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$15.50/250mg
507-20-0
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$16.00/25mL
10275-62-4
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20870-37-5
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Yield:10275-62-4 22% ，20870-37-5 22%
Reaction Conditions:
Stage #1: naphthalene;tertiary butyl chloridewith aluminium trichloride at 40 - 45; for 1 h;
Stage #2: with nitric acid in acetic anhydride at 20; for 2 h;Further stages.;
References:
Quast, Helmut;Nuedling, Wolfgang;Klemm, Gerhard;Kirschfeld, Andreas;Neuhaus, Patrik;Sander, Wolfram;Hrovat, David A.;Borden, Weston Thatcher [Journal of Organic Chemistry,2008,vol. 73,# 13,p. 4956 - 4961]