3,6-Dichloro-4-iodopyridazine synthesis
- Product Name:3,6-Dichloro-4-iodopyridazine
- CAS Number:130825-13-7
- Molecular formula:C4HCl2IN2
- Molecular Weight:274.87
141-30-0
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Yield: 84%
Reaction Conditions:
Stage #1:3,6-dichlorpyridazine with zinc chloride-2,2,6,6-tetramethylpiperidin-1-ide lithium chloride complex in tetrahydrofuran at 25; for 0.5 h;Inert atmosphere;
Stage #2: with iodine in tetrahydrofuran for 0.5 h;Inert atmosphere;
References:
Mosrin, Marc;Knochel, Paul [Organic Letters,2009,vol. 11,# 8,p. 1837 - 1840] Location in patent:supporting information; experimental part
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1000210-73-0
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