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ChemicalBook CAS DataBase List 3,5-Bis(2-cyanoprop-2-yl)toluene
120511-72-0

3,5-Bis(2-cyanoprop-2-yl)toluene synthesis

7synthesis methods
-

Yield:120511-72-0 79%

Reaction Conditions:

with sodium hydride

Steps:


Preparation of 2,2 '-(5-methyl-1,3-phenylene)di(2-methylpropionitrile) 2Compound 2, 2,2'-(5-methyl-l,3-phenylene)di(2-methylpropionitrile), can be prepared according to the procedure in example 1 of patent EP 0296749 Bl, which is hereby incorporated by reference in its entirety, but in particular in respect of thepreparation of 2,2'-(5-methyl-l,3-phenylene)di(2-methylpropionitrile) 2. Yield: 79%. Melting point: 125-127°C.

References:

GENERICS [UK] LIMITED WO2006/836, 2006, A1 Location in patent:Page/Page column 2; 9-10; 14; Figure 2

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