3-(1H-imidazol-1-yl)propane-1,2-diol synthesis
- Product Name:3-(1H-imidazol-1-yl)propane-1,2-diol
- CAS Number:34793-28-7
- Molecular formula:C6H10N2O2
- Molecular Weight:142.16
288-32-4
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Yield:34793-28-7 88%
Reaction Conditions:
with 1,4-diaza-bicyclo[2.2.2]octane in 5,5-dimethyl-1,3-cyclohexadiene at 110; for 6 h;
Steps:
5 Example 5
118g of glycerol carbonate,68g imidazole, 186g xylene and 1g DABCO were put into the flask, heated to reflux at 110 ° C for 6 hours, and the upper layer solvent was separated while hot.Then vacuum distillation1- (2,3-dihydroxy) propylimidazole, yield 88%.
References:
CN110776464,2020,A Location in patent:Paragraph 0016
288-32-4
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556-52-5
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34793-28-7
30 suppliers
$38.00/250mg
288-32-4
1033 suppliers
$5.00/25g
96-24-2
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34793-28-7
30 suppliers
$38.00/250mg