(1S,3S,5S)-2-AZABICYCLO[3.1.0]HEXANE-3-CARBOXYLIC ACID synthesis
- Product Name:(1S,3S,5S)-2-AZABICYCLO[3.1.0]HEXANE-3-CARBOXYLIC ACID
- CAS Number:214193-13-2
- Molecular formula:C6H9NO2
- Molecular Weight:127.14
194594-23-5
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214193-13-2
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Yield:-
Steps:
Multi-step reaction with 5 steps
1: PPTS
2: NH4Cl / 150 °C / 20 - 100 Torr
3: 65 percent / Et2Zn / 1,2-dichloro-ethane; hexane / a) 0 deg C, 30 min, b) RT, 6 h
4: DMAP, Et3N / CH2Cl2
5: 1.) aq. LiOH, 2.) HCO2H / 1.) MeOH
References:
Hanessian, Stephen;Reinhold, Ulrich;Saulnier, Michel;Claridge, Stephen [Bioorganic and Medicinal Chemistry Letters,1998,vol. 8,# 16,p. 2123 - 2128]
194594-24-6
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214193-13-2
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178172-26-4
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$144.00/250mg
214193-13-2
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$65.00/2.5mg
![2-Azabicyclo[3.1.0]hexane-2,3-dicarboxylic acid, 2-(1,1-dimethylethyl) 3-ethyl ester, (1S,3S,5S)-](/CAS/GIF/214193-11-0.gif)
214193-11-0
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214193-13-2
29 suppliers
$65.00/2.5mg