2-Methylene-1,3-dioxepane synthesis
- Product Name:2-Methylene-1,3-dioxepane
- CAS Number:69814-56-8
- Molecular formula:C6H10O2
- Molecular Weight:114.14
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Yield:69814-56-8 97.4%
Steps:
14 EXAMPLE 14
EXAMPLE 14 The procedure was as in Example 12, except that 32.0 g (0.25 mol) of 2,6-dimethylcyclohexanol were used instead of the 3,3-dimethylbutan-2-ol. The conversion of 2-chloromethyl-1,3-dioxepane was 97.4% and the yield of 2-methylene-1,3-dioxepane was 87.9%.
References:
US5455361,1995,A
![2-BROMOMETHYL-[1,3]DIOXEPANE](/StructureFile/ChemBookStructure3/GIF/CB4290553.gif)
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