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ChemicalBook CAS DataBase List 2-HYDROXY-1,3,5-BENZENETRICARBALDEHYDE
81502-74-1

2-HYDROXY-1,3,5-BENZENETRICARBALDEHYDE synthesis

5synthesis methods
2-Hydroxybenzene-1,3,5-tricarbaldehyde is synthesized from phenol or 4-hydroxybenzaldehyde[1].
2-HYDROXY-1,3,5-BENZENETRICARBALDEHYDE synthesis pathway one
2-HYDROXY-1,3,5-BENZENETRICARBALDEHYDE synthesis pathway two
-

Yield:81502-74-1 65%

Reaction Conditions:

Stage #1:trifluoroacetic acid;phenol with hexamethylenetetramine at 125; for 20 h;
Stage #2: at 150; for 3 h;

References:

Kastrati, Agonist;Bochet, Christian G. [Journal of Organic Chemistry,2019,vol. 84,# 12,p. 7776 - 7785]

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