2-fluoroacrolein synthesis
- Product Name:2-fluoroacrolein
- CAS Number:13989-27-0
- Molecular formula:C3H3FO
- Molecular Weight:74.05
![Butane, 1,1'-[(2-fluoro-2-propenylidene)bis(oxy)]bis-](/CAS/20210111/GIF/66450-75-7.gif)
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Yield:13989-27-0 90%
Reaction Conditions:
with hydrogenchloride in water at 70; for 2 h;Temperature;
Steps:
3 Preparation of 2-fluoropropenal
To 1 - ((1-butoxy-2-fluoropropenyl) oxy) butane was added dropwise73 g (0.2 mol) of 10% hydrochloric acid,70 ° C for 2 hours, after the completion of the reaction distillation,2-fluoropropenal is obtained. Yield 90%.
References:
CN107417524,2017,A Location in patent:Paragraph 0058; 0059; 0060; 0061; 0062-0067
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