2-(DIETHYLAMINOMETHYL)-BROMOBENZENE synthesis
- Product Name:2-(DIETHYLAMINOMETHYL)-BROMOBENZENE
- CAS Number:91428-19-2
- Molecular formula:C11H16BrN
- Molecular Weight:242.16
Yield:-
Reaction Conditions:
in toluene at 20; for 14 h;
Steps:
229.229A Preparation of (2-Bromo-benzyl)-diethyl-amine
To 1-Bromo-2-bromomethyl-benzene (2.17 g, 0.008 mmol) in toluene (15 mL) was added diethylamine (3.05 mL) and the mixture was stirred at room temperature for 14 hours. The reaction mixture was filtered and concentrated to give Example 229A as an oil.
References:
US2005/250753,2005,A1 Location in patent:Page/Page column 65
76041-86-6
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91428-19-2
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