2-CHLOROTETRAFLUOROPROPANOYL CHLORIDE synthesis
1synthesis methods
- Product Name:2-CHLOROTETRAFLUOROPROPANOYL CHLORIDE
- CAS Number:6066-46-2
- Molecular formula:C3Cl2F4O
- Molecular Weight:198.93
Yield:6066-46-2 6% ，24503-62-6 63%
Reaction Conditions:
with sulfuric acid;sulfur trioxide;silver nitrate;mercury(II) oxide for 8 h;Heating;Title compound not separated from byproducts;
References:
Kvicala, J.;Paleta, O.;Dedek, V. [Journal of Fluorine Chemistry,1990,vol. 47,# 3,p. 441 - 457]