2-(Chloromethyl)pyridine hydrochloride synthesis
- Product Name:2-(Chloromethyl)pyridine hydrochloride
- CAS Number:6959-47-3
- Molecular formula:C6H7Cl2N
- Molecular Weight:164.03
586-98-1
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$6.00/10g
6959-47-3
365 suppliers
$7.00/10g
Yield:6959-47-3 100%
Reaction Conditions:
with thionyl chloride
Steps:
Synthesis of 2-(chloromethyl)pyridine hydrochloride
Synthesis of 2-(chloromethyl)pyridine hydrochloride
2-pyridinylmethanol (100 g, 0.92 mol) was added under stirring and cooling (0°C) to 300 ml (4.1 mol) of SOCl2 during 2h.
The solution obtained was refluxed for 1h.
Then the excess of SOCl2 was removed in vacuum and the solid residue was used in the next stage as it is.
Yield 100%.
References:
Basell Polyolefine GmbH;Richter-Lukesova, Lenka;Mihan, Shahram;Fantinel, Fabiana;Nifant'ev, Ilya Eduardovich EP2606970, 2013, A1 Location in patent:Page/Page column
109-06-8
413 suppliers
$16.00/25g
87-90-1
464 suppliers
$10.00/10g
6959-47-3
365 suppliers
$7.00/10g
109-06-8
413 suppliers
$16.00/25g
6959-47-3
365 suppliers
$7.00/10g