ChemicalBook CAS DataBase List 2-Chloro-N4-(2-methypropyl)-3,4-quinolinediamine

2-Chloro-N4-(2-methypropyl)-3,4-quinolinediamine synthesis

5synthesis methods

Product Name:2-Chloro-N4-(2-methypropyl)-3,4-quinolinediamine
CAS Number:133860-76-1
Molecular formula:C13H16ClN3
Molecular Weight:249.74

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2-Chloro-N4-(2-methypropyl)-3,4-quinolinediamine

133860-76-1
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 17.8 g / Et₃N / CH₂Cl₂ / 0.5 h / Heating
2: H₂; MgSO₄ / Pt/C / ethyl acetate / 2585.74 Torr

References:

Gerster, John F.;Lindstrom, Kyle J.;Miller, Richard L.;Tomai, Mark A.;Birmachu, Woubalem;Bomersine, Shannon N.;Gibson, Shiela J.;Imbertson, Linda M.;Jacobson, Joel R.;Knafla, Roy T.;Maye, Peter V.;Nikolaides, Nickolas;Oneyemi, Folakemi Y.;Parkhurst, Gwen J.;Pecore, Sharon E.;Reiter, Michael J.;Scribner, Lisa S.;Testerman, Tracy L.;Thompson, Natalie J.;Wagner, Tammy L.;Weeks, Charles E.;Andre, Jean-Denis;Lagain, Daniel;Bastard, Yvon;Lupu, Michel [Journal of Medicinal Chemistry,2005,vol. 48,# 10,p. 3481 - 3491]