2-CHLORO-5-(FLUOROSULFONYL)BENZOIC ACID synthesis
- Product Name:2-CHLORO-5-(FLUOROSULFONYL)BENZOIC ACID
- CAS Number:21346-66-7
- Molecular formula:C7H4ClFO4S
- Molecular Weight:238.62
118-91-2
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: chlorosulfonic acid / 1 h / 120 °C / Inert atmosphere
2: potassium hydrogen bifluoride / 1,4-dioxane; water / 0.5 h / 20 °C / Inert atmosphere
References:
Grimster, Neil P.;Connelly, Stephen;Baranczak, Aleksandra;Dong, Jiajia;Krasnova, Larissa B.;Sharpless, K. Barry;Powers, Evan T.;Wilson, Ian A.;Kelly, Jeffery W. [Journal of the American Chemical Society,2013,vol. 135,# 15,p. 5656 - 5668]
137-64-4
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$31.00/250 mg
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