2-(azidomethyl)-4-methoxy-3,5-dimethylpyridine synthesis

2synthesis methods

Product Name:2-(azidomethyl)-4-methoxy-3,5-dimethylpyridine
CAS Number:913624-57-4
Molecular formula:C9H12N4O
Molecular Weight:192.22

2-Pyridinemethanol, 4-methoxy-3,5-dimethyl-, 2-methanesulfonate

477585-18-5
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2-(azidomethyl)-4-methoxy-3,5-dimethylpyridine

913624-57-4
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Yield:913624-57-4 100 mg

Reaction Conditions:

with sodium azide in N,N-dimethyl-formamide at 60; for 8 h;Inert atmosphere;

References:

Büll, Christian;Heise, Torben;van Hilten, Niek;Pijnenborg, Johan F. A.;Bloemendal, Victor R. L. J.;Gerrits, Lotte;Kers-Rebel, Esther D.;Ritschel, Tina;den Brok, Martijn H.;Adema, Gosse J.;Boltje, Thomas J. [Angewandte Chemie - International Edition,2017,vol. 56,# 12,p. 3309 - 3313][Angew. Chem.,2017,vol. 129,# 12,p. 3357 - 3361] Location in patent:supporting information

86604-78-6 Synthesis

3,5-Dimethyl-4-methoxy-2-pyridinemethanol

86604-78-6
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$7.00/5g

913624-57-4
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References