ChemicalBook CAS DataBase List 2,5-dichloroanilinium chloride

2,5-dichloroanilinium chloride synthesis

5synthesis methods

Product Name:2,5-dichloroanilinium chloride
CAS Number:33663-41-1
Molecular formula:C6H6Cl3N
Molecular Weight:198.4775

33663-41-1
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68-11-1 Synthesis

68-11-1
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$12.00/25g

6274-27-7
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Yield:6274-27-7 54%

Reaction Conditions:

Stage #1: 2,5-dichloroaniline hydrochloridewith sodium nitrite at 10; for 1 h;Diazotization;
Stage #2: mercaptoacetic acidwith hydrogenchloride;copper(II) sulfate at 20 - 50;Substitution;

References:

D'Andrea, Stan V.;Bonner, Daniel;Bronson, Joanne J.;Clark, Junius;Denbleyker, Ken;Fung-Tomc, Joan;Hoeft, Shelley E.;Hudyma, Thomas W.;Matiskella, John D.;Miller, Raymond F.;Misco, Peter F.;Pucci, Michael;Sterzycki, Roman;Tsai, Yuan;Ueda, Yasutsuga;Wichtowski, John A.;Singh, Janak;Kissick, Thomas P.;North, Jeffery T.;Pullockaran, Annie;Humora, Michael;Boyhan, Brenda;Vu, Truc;Fritz, Alan;Heikes;Fox, Rita;Godfrey, Jollie D.;Perrone, Robert;Kaplan, Murray;Kronenthal, David;Mueller, Richard H. [Tetrahedron,2000,vol. 56,# 31,p. 5687 - 5698]

33663-41-1
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