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ChemicalBook CAS DataBase List 2-(4-FLUOROPHENYL)-4,6-DIPHENYLPYRIDINE
91232-30-3

2-(4-FLUOROPHENYL)-4,6-DIPHENYLPYRIDINE synthesis

6synthesis methods
-

Yield:91232-30-3 79%

Reaction Conditions:

Stage #1: 3-(4-fluorophenyl)-1-phenylprop-2-yn-1-one;rac-methylbenzylamine in dimethyl sulfoxide at 20; for 1 h;Schlenk technique;Michael Addition;
Stage #2: with potassium tert-butylate in dimethyl sulfoxide at 100; for 12 h;regioselective reaction;

References:

Shen, Jinhai;Cai, Dingding;Kuai, Changsheng;Liu, Yunqi;Wei, Ming'E;Cheng, Guolin;Cui, Xiuling [Journal of Organic Chemistry,2015,vol. 80,# 13,p. 6584 - 6589]