2,4-DIFLUORO-3-IODO-PYRIDINE synthesis
- Product Name:2,4-DIFLUORO-3-IODO-PYRIDINE
- CAS Number:837364-88-2
- Molecular formula:C5H2F2IN
- Molecular Weight:240.98
3512-17-2
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837364-88-2
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Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: BuLi / tetrahydrofuran; hexane / 0.75 h / -100 °C
1.2: 84 percent / tetrahydrofuran; hexane / cooling
2.1: 98 percent / H2NNH2*H2O / tetrahydrofuran / 2 h / 50 °C
3.1: 89 percent / CuSO4*5H2O / H2O / 2 h / Heating
4.1: 93 percent / ICl
References:
Schlosser, Manfred;Bobbio, Carla;Rausis, Thierry [Journal of Organic Chemistry,2005,vol. 70,# 7,p. 2494 - 2502]
34941-90-7
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837364-88-2
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837364-97-3
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837364-95-1
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![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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837364-88-2
113 suppliers
$21.00/100mg