2,4,6-Tribromoaniline synthesis
- Product Name:2,4,6-Tribromoaniline
- CAS Number:147-82-0
- Molecular formula:C6H4Br3N
- Molecular Weight:329.81
synthesis-of-2-4-6-tribromoaniline-from-aniline
615-36-1
419 suppliers
$10.00/5g
147-82-0
218 suppliers
$19.00/10g
Yield:147-82-0 90%
Reaction Conditions:
with dibromamine-T in acetonitrile at 20; for 0.166667 h;
Steps:
2, 4, 6-Tribromoaniline
General procedure: TsNBr2 (1 mmol) was added at 0 C to a solution of the aromatic compound(1 mmol) in acetonitrile (2 mL). After 10 min of stirring at room temperature, sodium thiosulfate (200 mg approx.) was added and stirred for 10 min. The reaction wastaken up in ethyl acetate, dried over NaSO4, and concentrated. The crude productwas purified by flash chromatography or silica gel (230-400 mesh) with a mixtureof petroleum ether and ethyl acetate as eluent.
References:
Saikia, Indranirekha;Chakraborty, Pranita;Sarma, Manas Jyoti;Goswami, Mridusmita;Phukan, Prodeep [Synthetic Communications,2015,vol. 45,# 2,p. 211 - 217]
106-40-1
487 suppliers
$12.00/5g
147-82-0
218 suppliers
$19.00/10g
62-53-3
678 suppliers
$10.00/1g
147-82-0
218 suppliers
$19.00/10g
615-57-6
186 suppliers
$9.00/1g
147-82-0
218 suppliers
$19.00/10g
62-53-3
678 suppliers
$10.00/1g
615-57-6
186 suppliers
$9.00/1g
147-82-0
218 suppliers
$19.00/10g
106-40-1
487 suppliers
$12.00/5g