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ChemicalBook CAS DataBase List 2,4,5-TRICHLOROACETANILIDE
23627-24-9

2,4,5-TRICHLOROACETANILIDE synthesis

12synthesis methods
-

Yield: 99%

Reaction Conditions:

at 20 - 25;

Steps:

39.a
2,4,5-trichloroaniline (10 g) was dissolved in acetic anhydride (50 mL) and stirred overnight at room temperature. The resulting solid was filtered and air dried to give N-(2,4,5-trichlorophenyl)acetamide as an off white solid (12 g, 99%). Rf=0.5 (1:1 EA/heptane).

References:

Soll, Mark David;Hir de Fallois, Loic Patrick Le;Huber, Scot Kevin;Lee, Hyoung Ik;Wilkinson, Douglas Edward;Jacobs, Robert Toms;Beck, Brent Christopher US2010/125089, 2010, A1 Location in patent:Page/Page column 47