2,4,5-TRICHLOROACETANILIDE synthesis
- Product Name:2,4,5-TRICHLOROACETANILIDE
- CAS Number:23627-24-9
- Molecular formula:C8H6Cl3NO
- Molecular Weight:238.5
108-24-7
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23627-24-9
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Yield: 99%
Reaction Conditions:
at 20 - 25;
Steps:
39.a
2,4,5-trichloroaniline (10 g) was dissolved in acetic anhydride (50 mL) and stirred overnight at room temperature. The resulting solid was filtered and air dried to give N-(2,4,5-trichlorophenyl)acetamide as an off white solid (12 g, 99%). Rf=0.5 (1:1 EA/heptane).
References:
Soll, Mark David;Hir de Fallois, Loic Patrick Le;Huber, Scot Kevin;Lee, Hyoung Ik;Wilkinson, Douglas Edward;Jacobs, Robert Toms;Beck, Brent Christopher US2010/125089, 2010, A1 Location in patent:Page/Page column 47
75-36-5
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23627-24-9
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$33.39/250mg
2621-62-7
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23627-24-9
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2150-93-8
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23627-24-9
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99310-47-1
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90048-73-0
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23627-24-9
18 suppliers
$33.39/250mg