2,4,4'-TRIBROMODIPHENYL ETHER synthesis
- Product Name:2,4,4'-TRIBROMODIPHENYL ETHER
- CAS Number:41318-75-6
- Molecular formula:C12H7Br3O
- Molecular Weight:406.9
106-41-2
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108-36-1
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41318-75-6
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$204.00/10mg
Yield: 82%
Reaction Conditions:
with montmorillonite K10 Clay for 0.5 h;Microwave irradiation;
Steps:
2 Preparation of BDE-28
1,3-dibromobenzene (2.34g, 0.01mol) and 4-bromophenol (3.44g, 0.02mol) was stirred in a beaker and mix, 34g of montmorillonite was added. After stirring the reaction mix again into a dedicated microwave the flask was heated for 30min under microwave 170W, cooling. After washing with 100mL of methylene chloride were collected the reaction solution was washed, vacuum distillation to give a colorless oil fully, column chromatography, to give a white solid 3.31 g, 82% yield.
References:
Shandong Analysis Beta Center;Ji Wenhua;Chen Xiangfeng;Zhao Rusong;Gao Qianshan;Geng Yanling;Wang Xiao CN104860799, 2016, B Location in patent:Paragraph 0032-0034
615-58-7
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![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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41318-75-6
40 suppliers
$204.00/10mg
101-84-8
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41318-75-6
40 suppliers
$204.00/10mg