2,3-dibromo-quinoxaline synthesis
- Product Name:2,3-dibromo-quinoxaline
- CAS Number:23719-78-0
- Molecular formula:C8H4Br2N2
- Molecular Weight:287.94
15804-19-0
205 suppliers
$11.00/5g
23719-78-0
18 suppliers
inquiry
Yield:23719-78-0 98%
Reaction Conditions:
with phosphorus pentabromide at 160; for 2 h;
Steps:
77.A
To compound 77a (3.Og, 18.5mmol) were added PBr5 (17g) and the solution was heated to 16O0C for 2h. Cooled to O0C and added ice and stirred for 30min. The solution was extracted with CH2CI2, washed with 1N NaOH, dried (MgSO4), filtered, and concentrated to give compound 77b (5.2g, 98%).
References:
WO2009/111442,2009,A1 Location in patent:Page/Page column 67-68
2423-66-7
17 suppliers
inquiry
6935-29-1
27 suppliers
$144.00/250mg
23719-78-0
18 suppliers
inquiry
36856-91-4
141 suppliers
$9.00/250mg
15804-19-0
205 suppliers
$11.00/5g
23719-78-0
18 suppliers
inquiry