2',2'-DIFLUORO-2'-DEOXYURIDINE synthesis
- Product Name:2',2'-DIFLUORO-2'-DEOXYURIDINE
- CAS Number:114248-23-6
- Molecular formula:C9H10F2N2O5
- Molecular Weight:264.18
143157-27-1
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114248-23-6
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Yield:114248-23-6 99%
Reaction Conditions:
with ammonia in methanol at 20; for 12 h;Temperature;
Steps:
54; 134; 177 Compound 68
Compound 68-3 was dissolved in NH3/MeOH (600 mL) and stirred overnight. The solvent was concentratedto give the residue, which was purified by silica gel column chromatography (5% MeOH in DCM) to give68-4 (12 g, 99%) as a white solid
References:
US2015/105341,2015,A1 Location in patent:Paragraph 0676; 1030; 1311
122111-03-9
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114248-23-6
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1201895-94-4
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114248-23-6
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95058-81-4
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114248-23-6
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1445381-44-1
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114248-23-6
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