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4863-59-6

(1R)-(+)-TRANS-PINANE synthesis

8synthesis methods
-

Yield:4863-59-6 95 %Spectr. ，4795-86-2 5 %Spectr.

Reaction Conditions:

with C19H42CoN2Si2;hydrogen in neat (no solvent) at 20; under 3000.3 Torr; for 18 h;Inert atmosphere;Schlenk technique;Glovebox;Overall yield = 100 %;

References:

Enachi, Andreea;Baabe, Dirk;Zaretzke, Marc-Kevin;Schweyen, Peter;Freytag, Matthias;Raeder, Jan;Walter, Marc D. [Chemical Communications,2018,vol. 54,# 98,p. 13798 - 13801] Location in patent:supporting information

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