1H-PYRROLO[2,3-B]PYRIDIN-5-OL synthesis
- Product Name:1H-PYRROLO[2,3-B]PYRIDIN-5-OL
- CAS Number:98549-88-3
- Molecular formula:C7H6N2O
- Molecular Weight:134.14
![5-Benzyloxy-1H-pyrrolo[2,3-b]pyridine](/CAS/20180702/GIF/1036007-71-2.gif)
1036007-71-2
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98549-88-3
307 suppliers
$8.00/250mg
Yield:98549-88-3 95.5%
Reaction Conditions:
with palladium on activated charcoal;hydrogen in methanol;
Steps:
8 Preparation of 5-hydroxy-7-azaindole
Add 22.4g of 5-benzyloxy-7-azaindole to the hydrogenation bottle, dissolve it with methanol, add 1.1g of palladium carbon, replace the air in the hydrogenation bottle with hydrogen, and then add hydrogen. Stop the reaction after the pressure in the bottle does not change The palladium carbon was removed by filtration, and the organic solvent was swirled to obtain a crude product, which was washed with n-heptane to obtain 12.8 g of a refined product with a yield of 95.5%
References:
CN110922404,2020,A Location in patent:Paragraph 0051-0054
![5-METHOXY-1H-PYRROLO[2,3-B]PYRIDINE](/CAS/GIF/183208-36-8.gif)
183208-36-8
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$7.00/100mg
98549-88-3
307 suppliers
$8.00/250mg
![5-BROMO-1-TRIISOPROPYLSILANYL-1H-PYRROLO[2,3-B]PYRIDINE](/CAS/GIF/858116-66-2.gif)
858116-66-2
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$55.00/250mg
98549-88-3
307 suppliers
$8.00/250mg
![5-BROMO-PYRROLO[2,3-B]PYRIDINE-1-CARBOXYLICACIDTERT-BUTYLESTER](/CAS/GIF/928653-80-9.gif)
928653-80-9
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$27.00/100mg
98549-88-3
307 suppliers
$8.00/250mg
754214-56-7
187 suppliers
$25.00/250mg
98549-88-3
307 suppliers
$8.00/250mg