午夜插插,噜噜噜影院,啪啪伊人网,欧美熟夫,景甜吻戏视频,男人强操性感蕾丝美女视频在线网站,日本美女跳舞视频

Welcome to chemicalbook!
Chinese English Japanese Germany Korea
400-158-6606
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

ChemicalBook CAS DataBase List 1H-Inden-1-amine,2,3-dihydro-6-methyl-(9CI)
361389-84-6

1H-Inden-1-amine,2,3-dihydro-6-methyl-(9CI) synthesis

1synthesis methods
24623-20-9 Synthesis
6-Methyl-1-indanone

24623-20-9
156 suppliers
$16.00/1g

-

Yield:-

Reaction Conditions:

Stage #1: 2,3-dihydro-6-methyl-1H-inden-1-onewith ammonium acetate;sodium cyanoborohydride in isopropyl alcohol; for 16 h;Heating / reflux;
Stage #2: with sodium hydroxide in water;isopropyl alcohol at 20;

Steps:

A

6-Methyl-indan-l-one, (Intermediate 2) (3.0 g, 20.0 mmol) in isopropanol (20 mL) was treated with sodiumcyanoborohydride(9.01 g, 143.5 mmol) and ammonium acetate (47.4 g, 615 mmol) and the reaction was refluxed for 16 hours. The mixture was cooled to room temperature and basified with sodium hydroxide (10 mL). The residue was isolated in a typical aqueous workup to give, 6-methyl-indan- 1-ylamine (Intermediate 3).

References:

WO2009/23757,2009,A1 Location in patent:Page/Page column 12-13

1H-Inden-1-amine,2,3-dihydro-6-methyl-(9CI) Related Search: