(2,4-Dioxo-thiazolidin-3-yl)-acetic acid methyl ester synthesis
- Product Name:(2,4-Dioxo-thiazolidin-3-yl)-acetic acid methyl ester
- CAS Number:18345-22-7
- Molecular formula:C6H7NO4S
- Molecular Weight:189.19
Yield:18345-22-7 90%
Reaction Conditions:
Stage #1: 2,4-thiazolidinedionwith sodium hydride in tetrahydrofuran;mineral oil at 20;
Stage #2: bromoacetic acid methyl ester in tetrahydrofuran;mineral oil; for 3 h;Cooling with ice;Reflux;
References:
Nishida, Sho;Maruoka, Hiroshi;Yoshimura, Yuki;Goto, Takao;Tomita, Ryoko;Masumoto, Eiichi;Okabe, Fumi;Yamagata, Kenji;Fujioka, Toshihiro [Journal of Heterocyclic Chemistry,2012,vol. 49,# 2,p. 303 - 309] Location in patent:experimental part
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