bicyclo[2.2.2]oct-7-ene-2,3,5,6-tetracarboxylic acid synthesis
- Product Name:bicyclo[2.2.2]oct-7-ene-2,3,5,6-tetracarboxylic acid
- CAS Number:16672-29-0
- Molecular formula:C12H12O8
- Molecular Weight:284.22
![4,8-Etheno-1H,3H-benzo[1,2-c:4,5-c']difuran-1,3,5,7-tetrone, 3a,4,4a,7a,8,8a-hexahydro-, (3aα,4α,4aβ,7aα,8α,8aβ)-](/CAS/20210305/GIF/765302-31-6.gif)
765302-31-6
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16672-29-0
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Yield:-
Reaction Conditions:
with dmap in water; for 1 h;Reflux;
Steps:
2
Into a 200 mL glass flask, 10 g of BTA, 0.05 g of 4-dimethylaminopyridine and 100 g of distilled water were charged, refluxed for 1 hour with stirring, and cooled to give bicyclo [2.2.2] oct-7-ene-2 , 3,5,6-tetracarboxylic acid aqueous solution was obtained.
References:
JP5666076,2015,B2 Location in patent:Paragraph 0247