4,8-bis((2-ethylhexyl)oxy)benzo[1,2-b:4,5-b']dithiophene-2,6-dicarbaldehyde synthesis
- Product Name:4,8-bis((2-ethylhexyl)oxy)benzo[1,2-b:4,5-b']dithiophene-2,6-dicarbaldehyde
- CAS Number:1648615-16-0
- Molecular formula:C28H38O4S2
- Molecular Weight:502.73
32281-36-0
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: zinc; sodium hydroxide / water / 1 h / Reflux
1.2: 8 h / Reflux
2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 - -10 °C / Inert atmosphere
2.2: 0.5 h / -78 °C / Inert atmosphere
References:
Si, Peng;Liu, Jialei;Deng, Guowei;Huang, Heyan;Xu, Huajun;Bo, Shuhui;Qiu, Ling;Zhen, Zhen;Liu, Xinhou [RSC Advances,2014,vol. 4,# 49,p. 25532 - 25539]
18908-66-2
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1648615-16-0
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