3-De[(2,6-dideoxy-3-C-methyl-3-O-methyl-a-L-ribo-hexopyranosyl)oxy]-10,11-didehydro-11-deoxy-6-O-methyl-3-oxo-erythromycin 2'-acetate synthesis
- Product Name:3-De[(2,6-dideoxy-3-C-methyl-3-O-methyl-a-L-ribo-hexopyranosyl)oxy]-10,11-didehydro-11-deoxy-6-O-methyl-3-oxo-erythromycin 2'-acetate
- CAS Number:160145-82-4
- Molecular formula:C32H53NO10
- Molecular Weight:611.76
143353-81-5
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: pyridine / dichloromethane / 23 h / 0 - 20 °C
2: N-chloro-succinimide; thioformaldehyde / dichloromethane / 3.5 h / -5 °C
3: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetone / 14 h / Reflux
References:
Wei, Xin;You, Qidong [Organic Process Research and Development,2006,vol. 10,# 3,p. 446 - 449]
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