3,5-PYRIDINEDICARBOXYLIC ACID, 4-(1,3-BENZODIOXOL-5-YL)-1,4-DIHYDRO-2,6-DIMETHYL-, DIETHYL ESTER synthesis
- Product Name:3,5-PYRIDINEDICARBOXYLIC ACID, 4-(1,3-BENZODIOXOL-5-YL)-1,4-DIHYDRO-2,6-DIMETHYL-, DIETHYL ESTER
- CAS Number:10354-29-7
- Molecular formula:C20H23NO6
- Molecular Weight:373.4
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Yield:10354-29-7 95%
Reaction Conditions:
with iron supported on copper/Zeolite Socony Mobil-5 nanocatalyst in water at 20;Sonication;Hantzsch Dihydropyridine Synthesis;
Steps:
General procedure for preparation of Hantzsch1,4-dihydropyridine (DHP) derivatives 5(a-f)
General procedure: In a typical experiment, aromatic aldehyde (1 mmol), bketoester(2 mmol), ammonium acetate (1 mmol), and Fe-Cu/ZSM-5 (3 wt%) in 2 ml water were introduced in a 20-mL heavy-walled pear-shaped two-necked flask with nonstandard-tapered outer joint. The flask was attached to a12-mm tip diameter probe, and the reaction mixture was sonicated at ambient temperature at 20 % power of the processor. After completion of the reaction (monitored byTLC, within 5-8 min), the solid product was filtered,washed with water and ethanol, dried, and recrystallized from ethanol. The supported reagent was washed thrice with water and ethanol and dried under vacuum before reuse.
References:
Safa, Kazem D.;Esmaili, Maryam;Allahvirdinesbat, Maryam [Journal of the Iranian Chemical Society,2016,vol. 13,# 2,p. 267 - 277]
120-57-0
5 suppliers
$28.39/25g
7664-41-7
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$15.00/100ml
141-97-9
796 suppliers
$5.00/25g
10354-29-7
7 suppliers
inquiry
