4-(2-chloro-4-pyrimidinyl)benzoic acid methyl ester synthesis
- Product Name:4-(2-chloro-4-pyrimidinyl)benzoic acid methyl ester
- CAS Number:1026029-33-3
- Molecular formula:C12H9ClN2O2
- Molecular Weight:248.67
3934-20-1
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Yield:1026029-33-3 85%
Reaction Conditions:
with bis-triphenylphosphine-palladium(II) chloride;sodium carbonate in 1,4-dioxane;water;N,N-dimethyl-formamide at 80; for 10 h;Inert atmosphere;
References:
Bliss, Brian I.;Ahmed, Feryan;Iyer, Subashree;Lin, Weimin;Walker, Joel;Zhao, He [Tetrahedron Letters,2010,vol. 51,# 25,p. 3259 - 3262] Location in patent:supporting information; experimental part